Practical Scanning Electron Microscopy: Electron and Ion Microprobe Analysis

Copertina anteriore
Joseph Goldstein
Springer Science & Business Media, 6 dic 2012 - 582 pagine
In the spring of 1963, a well-known research institute made a market survey to assess how many scanning electron microscopes might be sold in the United States. They predicted that three to five might be sold in the first year a commercial SEM was available, and that ten instruments would saturate the marketplace. In 1964, the Cambridge Instruments Stereoscan was introduced into the United States and, in the following decade, over 1200 scanning electron microscopes were sold in the U. S. alone, representing an investment conservatively estimated at $50,000- $100,000 each. Why were the market surveyers wrongil Perhaps because they asked the wrong persons, such as electron microscopists who were using the highly developed transmission electron microscopes of the day, with resolutions from 5-10 A. These scientists could see little application for a microscope that was useful for looking at surfaces with a resolution of only (then) about 200 A. Since that time, many scientists have learned to appreciate that information content in an image may be of more importance than resolution per se. The SEM, with its large depth of field and easily that often require little or no sample prepara interpreted images of samples tion for viewing, is capable of providing significant information about rough samples at magnifications ranging from 50 X to 100,000 X. This range overlaps considerably with the light microscope at the low end, and with the electron microscope at the high end.
 

Sommario

Chapter I
1
Depth of Field
6
Combination SEMEPMA
14
Electron Optics
21
Electron Lenses
29
Electron Probe Diameter d vs Electron Probe Current i
40
Chapter III
41
Electron BeamSpecimen Interaction
49
Solid State XRay Detectors
274
A Comparison of Crystal Spectrometers with Solid State
281
The Analysis of XRay Spectral Data
285
Chapter VIII
299
Characterizing the XRayExcited Volume
305
Chapter IX
326
Atomic Number Correction kz
343
Summary Discussion of the ZAF Method
350

Emitted ElectronsBackscattered Electrons
57
Emitted ElectronsLowEnergy Electrons
64
Auger Electrons
72
Chapter IV
78
Image Formation in the Scanning Electron
95
A EverhartThornley Detector
101
A Signal Limitations
115
B Resolution Limitation due to BeamSpecimen Interactions
124
Image Defects
143
Contrast Mechanisms of Special Interest
149
Magnetic Contrast in the SEM
180
Voltage Contrast
198
Specimen Preparation Special Techniques
211
Dynamic Experiments in the SEM
220
Applications of the SEM
228
Examination of Magnetically Written Information with
247
XRay Spectral Measurement
263
The Empirical Method for Quantitative Analysis
352
Computational Schemes for Quantitative XRay
373
Data Reduction Based on the Hyperbolic Method
388
Chapter XI
400
Specimen Preparation for Quantitative Analysis
418
Applications Involving Compositional Analysis
426
Special Techniques in the XRay Analysis
435
Precision and Sensitivity in XRay Analysis
443
Soft XRay Emission Spectra
465
Chapter XIII
488
Analysis
514
Summary
524
Ion Microprobe
532
Qualitative Analysis
541
Quantitative Analysis
548
Index
573
Copyright

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